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नाइट्रिक अम्ल और सल्फ्यूरिक अम्ल के मिश्रण में फेरस सल्फेट विलयन मिलाते हैं |

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`"2HNO"_(3)+6"FeSO"_(4)+3"H"_(2)"SO"_(4)to 3"Fe"_(2)("SO"_(4))_(3)+2"NO"+4"H"_(2)"O"`

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