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सोडियम सल्फाइड तथा सोडियम सल्फेट के विलयन में `I_2` मिलाकर गर्म करते हैं।

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सोडियम थायोसल्फेट (हाइपो या `Na_2S_2O_3`) बनता है।
`Na_2S + Na_2 SO_3 + I_2 oversetDeltato Na_2 S_2 O_3 + 2Nal`

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